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我们利用分子束外延方法生长了低温GaAs薄膜,并应用X射线双晶衍射、TEM等手段对其进行了初步研究.发现原生样品和树底之间存在晶格失配.随着退火温度的上升,晶格失配逐渐消失.TEM观察到600,700,850℃退火后的样品中存在大量的砷沉淀物.沉淀物大致呈球形.砷沉淀物的直径随着退火温度的上升而线性地增大,而密度却随退火温度的上升指数地下降.
We use molecular beam epitaxy growth of low-temperature GaAs thin film, and the application of X-ray double crystal diffraction, TEM and other means to conduct a preliminary study. There was a lattice mismatch between the native sample and the tree bottom. As the annealing temperature increases, the lattice mismatch gradually disappears. TEM showed that a large amount of arsenic was present in the samples annealed at 600, 700, and 850 ° C. The precipitate is roughly spherical. The diameter of arsenic precipitates increases linearly with increasing annealing temperature, whereas the density decreases exponentially with increasing annealing temperature.