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TiB2/ZL114 composites with the density of 2.733 g/cm3 were fabricated through reaction of K2TiF4 and KBF4 (LSM method). The composites were characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). The intal friction measurements were performed on DTM-Ⅱ-J dynamic modulus damping an-alyzer and the mechanisms were investigated. Experimental results indicate that reinforced particles are well-distributed in the matrix and the intal friction value of TiB2/ZL114 composites is up to a maximum of 9.04x10-3, almost twice that of ZL114. The intal friction results form dislocation vibration within the material,the sliding of grain boundary and phase interface, and together with the micro-plastic deformation caused by difference in coefficients of thermal expansion and elasticity modulus of various phases. The average intal friction values of samples with the sizes of 40 min×4 mm×2 mm, 40 mm×8 mm×2 mm and 40 mm×25 mm×2 mm are 8.83x 10-3, 8.89x 10-3, and 8.93×10-3, respectively. Thus, the developed composites are of low density, high intal friction, and the sizes of samples have no relation to the intal friction behavior.