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在我国许多高等学校和科学研究机关都先后建立了 X 射线晶体分析实验室,几乎每个实验室都有粉末法的照相设备,从事各方面的研究。关于 X 射线粉末法的原理、方法、操作技术和具体步骤,本刊已有介绍。近年来苏联、英、美等国也都有专书出版,详细介绍有关这方面的问题。本文主要通过实例阐述粉末法在无机化学研究中的具体应用。
Many of our colleges and universities and scientific research institutes have established X-ray crystal analysis laboratories. Almost every laboratory has a powder-based photographic equipment and is engaged in various aspects of research. X-ray powder method on the principles, methods, operating techniques and specific steps, the publication has been introduced. In recent years, the Soviet Union, Britain, the United States and other countries have also published special books detailing relevant issues in this regard. This article mainly expounds the concrete application of powder method in inorganic chemistry research through examples.