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以5-氨基-1,3-苯二甲酸和对叔丁基苯甲酰肼为原料合成了一种新型电致磷光材料中间体5-溴-1,3-二[2-(4′-叔丁基苯基)-1,3,4-(噁二唑基-5)]苯,探讨了反应条件对合成反应的影响,反应的总收率为20.0%,方法可行。
A novel phosphorescent material was synthesized from 5-amino-1,3-benzenedicarboxylic acid and p-tert-butylbenzoic hydrazide. 5-Bromo-1,3-bis [2- Tert-butylphenyl) -1,3,4- (oxadiazolyl-5)] benzene. The effects of reaction conditions on the synthesis were discussed. The total yield of the reaction was 20.0%. The method was feasible.