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Tordylium apulum为一种生长于地中海和西亚地区的一年生草本植物。将其干燥后分成两份,一份(334g)用甲醇提取,而后用乙醚和丙酮处理,得A-E(8g)和A-A(2.2g),A-E用硅胶柱色谱以递增极性洗脱,得到335个组分,组分109～113经制备型薄层色谱分离得A1,组分114～139中分离得A2,组分150～210中经柱色谱分离得A3,组分317～335中经制备型薄层色谱
Tordylium apulum is an annual herb that grows in the Mediterranean and Western Asia. After drying, it was divided into two portions. One portion (334 g) was extracted with methanol and then treated with ether and acetone to obtain AE (8 g) and AA (2.2 g). The AE was eluted with increasing polarity on a silica gel column chromatography to obtain 335 Components, components 109 to 113 were separated by preparative thin layer chromatography to obtain A1, components 114 to 139 were separated to A2, components 150 to 210 were separated by column chromatography to obtain A3, and components 317 to 335 were prepared Thin layer chromatography