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应用ＴＬＣＳ法测定利脑心胶囊中芍药甙含量．样品用甲醇提取、大孔吸附树脂分离芍药甙，以硅胶Ｇ为薄层吸附剂，苯－甲醇－醋酸乙酯－氨水（１０：４：２：０．５）为展开剂，茴香醛－冰醋酸－硫酸（０．１：１０：０．２）溶液为显色剂，用ＣＳ－９３０薄层扫描仪，在λｓ＝５５５ｎｍ，λＲ＝６７０ｎｍ波长处测定含量。本法平均加样回收率为１００．５％，ＲＳＤ为３．７６％（ｎ＝５）。
The content of paeoniflorin in Li Nao Xin capsules was determined by TLCS. The sample was extracted with methanol, macroporous adsorption resin was used to separate peony oxime, silica gel G was used as thin layer adsorbent, and benzene-methanol-ethyl acetate-ammonia water (10:4:2:0.5) was used as developing solvent. Anisaldehyde-ice The acetic acid-sulfuric acid (0.1:10:0.2) solution was used as a color developer. The content was measured at a wavelength of λs=555 nm and a wavelength of λR=670 nm using a CS-930 thin layer scanner. The average recovery rate of this method is 100.5%, and the RSD is 3.76% (n=5).