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通过对尿碘测定方法标准化工作小组提供的方法框架的验证表明，该方法的线性范围为０～３００μｇ／Ｌ，相关系数｜ｒ｜＜０．９９９０。对碘浓度为５５．５，１５１．７，２０９．４μｇ／Ｌ的三种尿样，６次重复测定的变异系数均小于６％，样品加标回收实验的平均回收率为９８．２％。对尿碘外质控样的测定值与标示量吻合。尿样保存两周内以４℃冷藏为佳。方法在现场应用中，所测尿碘的中位数及频数分步布与该地区供碘情况符合。该方法灵敏、准确、易于操作，稳定性、适用性均满足生物材料分析方法研制准则要求，便于推广。
Validation of the methodological framework provided by the Working Group on Standardization of Urine Determination Methods showed that the linear range of this method was 0-300 μg / L with a correlation coefficient | r | <0.9990. For the three urine samples with iodine concentrations of 55.5, 151.7 and 209.4 μg / L, the coefficients of variation of 6 replicates were all less than 6%. The average recoveries of the spiked samples were 98.2%. Urinary iodine external control sample measured values and labeled consistent. It is better to store the urine sample at 4 ° C within two weeks of storage. Methods In the field application, the median and frequency of urinary iodine measured by stepwise cloth were consistent with the situation of iodine supply in this area. The method is sensitive, accurate, easy to operate, stability and applicability meet the requirements of the guidelines for the development of biomaterials analytical methods, easy to promote.