【摘 要】
:
The crystal C28H42O12NP is the monoclinic space group P21, with a = 10. 158(1), b=9. 069(1), c=18. 147(3) A , β=90. 72(1)% V=1671. 6 A3, Mr=615. 61, Z=2, Dx=1
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The crystal C28H42O12NP is the monoclinic space group P21, with a = 10. 158(1), b=9. 069(1), c=18. 147(3) A , β=90. 72(1)% V=1671. 6 A3, Mr=615. 61, Z=2, Dx=1.23 g/cm3, μ=2.16 cm-1, F(000) = 660. The final R = 0. 071 and Rw = 0. 073 for 1860 observed reflections [I≥3σ(I)]. The results of structure analysis indicate that the configuration of the chiral carbon atom C(41) formed in the reaction is R *.
The crystal C28H42O12NP is the monoclinic space group P21, with a = 10. 158 (1), b = 9. 069 (1), c = 18.147 A, β = 90.72 (1)% V = 1671. 6 A3, Mr = 615.61, Z = 2, Dx = 1.23 g / cm3, μ = 2.16 cm-1 and F (000) = 660. The final R = 0. 071 and Rw = 0. 073 for 1860 observed reflections [I ≧ 3σ (I)]. The results of structure analysis indicate that the configuration of the chiral carbon atom C (41) formed in the reaction is R *.
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