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目的:建立抗病毒口服液中苦参碱含量测定的方法。方法:用三氯甲烷和氨水萃取,采用高效液相色谱法测定。色谱柱n为mE,c柱lip温se为X3D0B℃-C。18柱结,果流:动苦相参为碱乙检腈测-浓磷度酸在盐0缓.0冲09液～(0p.1H86m.8g·,Vm/LV-=1范25围∶7内5)与,进峰样面量积为积1分0值μL呈,流良速好为的1线.0性m关L·系m(inr=-1,0检.99测9波6)长;平为均21加0样回收率为100.89%,RSD=0.497%。结论:本方法准确、灵敏度高、重复性好,可用于抗病毒口服液的质量控制。
Objective: To establish a method for determination of matrine in anti-viral oral solution. Methods: Extraction with trichloromethane and ammonia, using high performance liquid chromatography. Column n is mE, c column lip temperature se is X3D0B ℃ -C. 18 column, fruit flow: bitter phase associated with alkali B nitrile test - concentrated acidity in the salt 0. Slow 0. 0 red 09 liquid ~ (0p.1H86m.8g ·, Vm / LV- = 1 range of Fan 25: 7 within 5) and, into the peak area of the product plot for the product of 1 points 0 μL was, the flow rate of good for the good 1 line .0 sex m off L · Department m (inr = -1,0 test .99 measured 9 Wave 6) long; flat average 21 plus 0 sample recovery was 100.89%, RSD = 0.497%. Conclusion: The method is accurate, sensitive and reproducible. It can be used for the quality control of antiviral oral liquid.