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对睾酮及表睾酮的三甲基硅烷化进行了详细考察,找到了较好的抗氧剂巯基乙醇,确定了较好的衍生化条件,衍生化产物单一。并采用GC-MS法测定了尿中睾酮与表睾酮的比值。实验条件为:以氦为载
The test of testosterone and epostereone trimethylsilylation were investigated in detail to find a better antioxidant mercaptoethanol, to determine a better derivatization conditions, derivatization of a single product. The ratio of testosterone in urine to epicastone testosterone was determined by GC-MS. Experimental conditions are: Helium is contained