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复方枸橼酸钠注射液又名抗凝剂(ACD)、血液保养液,为医疗单位常用的抗凝血药。该注射液类似处方较多,但国内医疗单位广泛使用处方Ⅰ〔沈阳药学院药剂教研室编.常用药物制剂.1979:585〕,我们应用改良 Miller 试剂,采用比色法测定 ACD 中的葡萄糖的含量经回收实验及样品测定,结果尚称满意。试药1.α-无水葡萄糖、苯酚、氢氧化钠、酒石酸钾钠、枸橼酸钠(AR)、无水亚硫酸钠、枸橼酸(CP)、3,5-二硝基水杨酸(LR)。2.改良 Miller 试剂(以下简称试剂):3,5-二硝基水杨酸1g,苯酚0.2g,亚硫酸钠
Compound sodium citrate injection, also known as anticoagulant (ACD), blood maintenance solution, commonly used for medical units anticoagulants. The injection of similar prescriptions more, but the widespread use of the domestic medical unit prescription 〔Shenyang Pharmaceutical College Pharmacy Teaching Department Editor. Commonly used pharmaceutical preparations .1979: 585〕, we use modified Miller reagent, the colorimetric determination of glucose in ACD After recovery experiments and sample determination, the results are still satisfied. Reagents 1. α-Anhydrous glucose, phenol, sodium hydroxide, potassium sodium tartrate, sodium citrate (AR), anhydrous sodium sulfite, citric acid (CP), 3,5-dinitrosalicylic acid LR). 2. Modified Miller reagent (hereinafter referred to as reagent): 3,5-dinitrosalicylic acid 1g, phenol 0.2g, sodium sulfite