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文章主要研究了在130 ℃±0.5℃的熔融尿素中应用交流示波极谱进行了无机去极剂离子Cu~(2+)、Cd~(2+)、Ni~(2+)和Co~(2+)及在水溶性和不溶性Ba~(2+)、Ca~(2+)的化合物的示波极谱特性.同时研究了在滴汞电极和Kaliskova电极上的硝基苯等有机化合物的吸附作用.进一步证实和扩充了文献[5]的研完工作,并进行定性的Q值测量及定性分布图,从而预示同时测定Cu~(2+)、Cd~(2+)、Ni~(2+)和Co~(2+)的定量分析的可能性.展示了硝基苯等有机化合物的分析可能性.对于水溶性和不溶性的化合物的定性和定量分析将是继续研究的课题.
In this paper, we investigated the effects of inorganic depolarizing agent ions Cu 2 +, Cd 2 +, Ni 2+ and Co ~ (2+) as well as the oscillopolarographic properties of water-soluble and insoluble Ba ~ (2 +) and Ca ~ (2+) compounds.Meanwhile, the effects of organic compounds such as nitrobenzene on the droplet mercury electrode and the Kaliskova electrode The further work is to confirm and extend the work done in [5] and carry out the qualitative Q value measurement and qualitative distribution map, which indicates that simultaneous determination of Cu 2+, Cd 2+, Ni 2+, (2+) and Co ~ (2+), demonstrating the possibility of analysis of organic compounds such as nitrobenzene, etc. The qualitative and quantitative analysis of water-soluble and insoluble compounds will continue to be a topic of study.