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采用中子活化分析相对＿Ｋ０法对研制的两个深海多金属结核标准物质ＧＳＰＮ＿２和ＧＳＰＮ＿３中的２６种主量和微量元素进行了定值测定，所得结果与初定值符合；对中子辐照自屏蔽效应进行了实验测定和理论计算，结果显示了很好的一致性；同时还对这两个多金属结核标准物中的Ａｓ、Ｂａ、Ｃｅ、Ｃｏ、Ｅｕ、Ｆｅ、Ｌａ、Ｌｕ、Ｍｎ、Ｍｏ、Ｎａ、Ｓｂ、Ｓｍ、Ｓｃ、Ｔｈ、Ｙｂ和Ｚｎ的取样量与取样误差关系进行了研究。结果表明，在ＧＳＰＮ＿２和ＧＳＰＮ＿３试样中分别有８种和１１种元素，在取样量１０ｍｇ时其取样误差小于１％。
The determination of 26 major and trace elements in two deep-sea polymetallic nodules, GSPN_2 and GSPN_3, developed by neutron activation analysis relative_K0 method, was consistent with the initial values. For neutron irradiation The self-shielding effects were experimentally determined and calculated theoretically, and the results showed good agreement. Meanwhile, the contents of As, Ba, Ce, Co, Eu, Fe, La, Lu and Mn in the two polymetallic nodule standards , Mo, Na, Sb, Sm, Sc, Th, Yb and Zn were studied. The results showed that there were 8 and 11 elements in GSPN_2 and GSPN_3 respectively. The sampling error was less than 1% when the sample volume was 10mg.