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采用高效液相色谱法同时测定甲磺酸培氟沙星胶囊的含量。C18柱(Eclipse4.6mm×150mm);流动相:以0.05mol/L枸橼酸—乙腈(82∶18);检测波长276nm;流速1ml/min。线性范围为8~48μg/mlr=0.996(n=6);平均回收率99.8%,RSD为0.30%
Simultaneous Determination of Pefloxacin Mesylate Capsules by High Performance Liquid Chromatography. C18 column (Eclipse 4.6 × 150mm); mobile phase: 0.05mol / L citric acid-acetonitrile (82:18); detection wavelength 276nm; flow rate 1ml / min. The linear range was 8 ~ 48μg / mlr = 0.996 (n = 6). The average recovery was 99.8% with a RSD of 0.30%