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利用水热方法合成了超分子化合物(C10N2H9)3[PMo12O40]·3H2O,通过元素分析、ICP和X射线单晶衍射确定了其晶体结构,并通过IR和XRD进行了结构表征,采用热重分析和循环伏安曲线研究了晶体的热稳定性和氧化还原性．该化合物是由联吡啶、水以及[PMo12O40]3-阴离子组成,它们之间存在较强的氢键作用,自组装成超分子结构化合物．
The crystal structure of the supramolecular compound (C10N2H9) 3 [PMo12O40] · 3H2O was synthesized by hydrothermal method. The crystal structure was confirmed by elemental analysis, ICP and X-ray single crystal diffraction. The crystal structure was characterized by IR and XRD. The cyclic voltammograms were used to study the thermal stability and redox properties of the crystals. The compound is composed of bipyridine, water and [PMo12O40] 3-anions, which have strong hydrogen bonding and self-assemble into supramolecular compounds.