Synthesis and Crystal Structure of [H-amp]4[Mo8O26（DMF）2].2H2O（amp = 2-Amino-6-methyl-pyridine）

• 作 者: CHENZhen-Feng LIUBing LIANGHon
• 机 构: CollegeofChemistryandChemicalEngineering,CollegeofChemistryandChemicalEngineering,InstituteofOrganic
• 出 处: 结构化学
• 发表日期: 2004年1期
• 关键词: [H-amp]4[Mo8O26(DMF)2].2H2O 辛钼酸盐 合成 晶体结构 2-氨基-6-甲基嘧啶 N N-二甲基甲酰胺 octamolybdate s
• 基金项目: This work was supported by the Natural Science Foundation and the Youth Science Foundation of Guangxi province

The reaction of MoO2(acac)2 with 2-amino-6-methyl-pyridine (amp) in the mixedsolvent of DMF (N,N-dimethylformamide) and water affords the title complex [H-amp]4[Mo8026(DMF)2].2H20 which was characterized by elemental analysis, IR spectroscopy andsingle-cr