Influence of High Magnetic Field Annealing on Aicrostructure of Pulse-Electrodeposited Nanocrystalli

来源 :Journal of Iron and Steel Research(International) | 被引量 : 0次 | 上传用户:jiangxiaohui
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The effects of high magnetic field armealihng on the morphology and texture of pulsed-electrodeposited Co-Ni-P films were investigated by field emission scanning electronic microscopy(FE-SEM),atomic force microscopy(AFM)and X-ray diffraction(XRD).The as-deposited film with cluster structural on a rough surface changed into non-uniform and bigger nanocrystalline during the no-field annealing due to a recrystallization process.Post-deposition annealing under a magnetic field favored to form a more homogeneous surface with smaller grain size and lower roughness.The magneto-induced a mixed phase structure including fcc-Ni,hcp-Co and fcc-CoNiP appeared in the case of the films annealed at a 9T magnetic field.The possible overlapping effects such as diffusion and recrystallization obtained by the magnetic field annealing on the morphology evolution and on the phase transformation in the films were interpreted. The effects of high magnetic field armealihng on the morphology and texture of pulsed-electrodeposited Co-Ni-P films were investigated by field emission scanning electronic microscopy (FE-SEM), atomic force microscopy (AFM) and X-ray diffraction The as-deposited film with cluster structural on a rough surface changed into non-uniform and bigger nanocrystalline during the no-field annealing due to a recrystallization process. Post-deposition annealing under a magnetic field favored to form a more homogeneous surface with smaller grain size and lower roughness. The magneto-induced a mixed phase structure including fcc-Ni, hcp-Co and fcc-CoNiP was found in the case of the annealed at 9T magnetic field. by the magnetic field annealing on the morphology evolution and on the phase transformation in the films were interpreted.
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