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The ferrocenyl compound,N-phenylbis(ferrocenecarboxyl)imide (C28H23NO2Fe2,Mr=517.17),was synthesized and structurally characterized by means of X-ray single-crystal dif-fraction. It crystallizes in monoclinic,space group C2/c with a=21.374(14),b=10.430(7),c= 10.741(7) ,β=114.184(8)°,V=2184(2) 3,Z=4,Dc=1.573 g/cm3,F(000)=1064,μ(MoKα)= 1.355 mm–1,T=291(2) K,the final R=0.0548 and wR=0.1437 for 1524 observed reflections with I > 2σ(I). In this compound,the nitrogen atom links two ferrocenyl groups and one phenyl group forming a novel imido derivative.
It crystallizes in monoclinic, space group C2 / c with a = 1, and it has been found that the ferrocenyl compound of N-phenylbis (ferrocenecarboxyl) imide (C28H23NO2Fe2, Mr = 517.17) 21.374 (14), b = 10.430 (7), c = 10.741 7, β = 114.184 (8) °, V = 2184 (2) 3, Z = 4, Dc = 1.573 g / cm3, F In this compound, the final R = 0.0548 and wR = 0.1437 for 1524 observed reflections with I> 2σ (I). In this compound, the nitrogen atom links two ferrocenyl groups and one phenyl group forming a novel imido derivative.