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报道了标题化合物的合成,其结构经X-射线衍射分析得到了表征。化合物为单斜晶系,P21/c空间群,相关晶体数据为:a=1.3420(3)nm,b=0.9720(2)nm,c=0.7900(2)nm,β=92.00(3)°,V=1.0299(4)nm3,Z=4,Dc=1.429g/cm3,F(000)=456,μ=0.345nm-1,R=0.0435,wR=0.0894。晶体分子通过氢键以及分子间作用力相互连接在一起,形成超分子键,并通过氢键相互连接,形成三维网状结构,使分子结构更加趋于稳定。
The synthesis of the title compound was reported and its structure was characterized by X-ray diffraction analysis. The compounds are monoclinic and P21 / c space group with the related crystal data as follows: a = 1.3420 (3) nm, b = 0.9720 (2) nm, c = V = 1.0299 (4) nm3, Z = 4, Dc = 1.429 g / cm3, F (000) = 456, μ = 0.345 nm-1, R = 0.0435, wR = 0.0894. The crystal molecules are connected to each other through hydrogen bonds and intermolecular forces to form supramolecular bonds and are connected to each other through hydrogen bonds to form a three-dimensional network structure, which makes the molecular structure more stable.