A Novel Sample Introduction Technique for the Simultaneous Determination of As,Se,Ge and Hg in

• 出 处: Chemical Research in Chinese Universities
• 发表日期: 2001年04期
• 关键词: hydride simultaneous affecting generating digestion absolute surfactant behave R

A novel technique of Moveable Reduction Bed Hydride Generator（MRBHG）was applied tohe hydride generation or cold vapor generation of As，Se，Ge，and Hg existing In TraditionalChinese Medicinal Material（TCM）．The simultaneous determination of the multi－elements wasperformed with ICP－MS．A solid reduction system involving the use of potassiumtetraborohydride and tartaric acid was applied to generating metal hydride or cold vaporefficiently．The factors affecting the metal cold vapor generation were studied．The mainadvantage of the technique is that only a 4μL volume of sample was required for the cold vapor

A novel technique of Moveable Reduction Bed Hydride Generator (MRBHG) was applied to a hydride generation or cold vapor generation of As, Se, Ge, and Hg existing In Traditional Chinese Medicinal Material (TCM). The simultaneous determination of the multi-elements wasperformed with ICP-MS. A solid reduction system involving the use of potassium tetrachloride and tartaric acid was applied to generating metal hydride or cold vaporefficiently. The factors affecting the metal cold vapor generation were studied. The main advantage of the technique is that only only 4μL volume of sample was required for the cold vapor