Synthesis, Characterization and X-ray Structure of N-（4- bromobutanoyl-N＇-（2-3- and 4-methylphenyl）

• 作 者: Hamza M Abosadiya Siti Aishah
• 机 构: SchoolofChemicalSciencesandFoodTechnology
• 出 处: 结构化学
• 发表日期: 2015年3期
• 关键词: 甲基苯基 X射线结构 硫脲 合成 溴 分子间氢键 表征 X射线晶体学 4-bromobutyryl chloride thiourea derivatives
• 基金项目: The authors thank the Ministry of Higher Education of Malaysia and Universiti Kebangsaan Malaysia for the research grant DIP-2014-016and FRGS/1/2013/ST01/UKM/03/4. One of us HAMZA would like to thank

N-4-(bromobutanoyl)-N’-(o-, m- and p-tolyl)thioureas 3a, 3b and 3c respectively, were synthesized by the reaction of 4-bromobutanoylisothiocyanate with p-, m- and o-toludine. The products were characterized by IR, and NMR spectroscopic techniques. The two