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Transitional metal oxides [1-4] have long been considered as promising anode materials for lithium-ion batteries to improve the graphite anode, because they could gain much higher specific capacity and power density compared with the graphite-based anode.Uniform Co3O4/NiO nanowires with typical diameter of 200-500 nm and lengths of up to several micrometers have been synthesized through a convenient oxalate co-precipitation method and followed by a calcining process.