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A novel organic-inorganic hybrid based on saturated α-Keggin-type germanomolybdates with mixed ligands,namely,[NH4]2[H8L][Cu(PA)2][α-GeMo12O40]·8H2O(1)(HPA = 2-picolinic acid,H6L =1,3-bis[tris(hydroxymethyl)methylamino]propane)has been obtained via the conventional solution synthesis method and structurally characterized by elemental analyses,IR spectrum,thermogravimetric analyses,and single-crystal X-ray diffraction.