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In this paper,the sensing of Para-substitued Anilines in THz region has been reported by using terahertz time-domain spectroscopy(THz-TDS).Several aniline compounds,such as p-chloroaniline,p-toluidine,p-nitroaniline,p-methoxyaniline are researched here.The results show that the compounds have fingerprints in the region of 0.1–3 THz(3-100 cm-1).And all the spectra are correlated with the intermolecular interactions brought by the functional groups at the para-position of aniline compounds.