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Low Temperature Plasma Probe was studied and applied to act on the surface of samples,which were liquid or solid.With the use of a simple DBD probe producing low temperature plasma with a quartz tube to act on the liquid sample or to ablate solid sample directly with various probe in dimension.Disintegration of polysaccharide,including sucrose,maltose and lactose,by dielectric barrier discharge plasma in helium at atmospheric pressure were obtained by LTP-Probe-ion chromatography with liquid samples.