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Direct methanol fuel cells(DMFCs)has been extensively studied to develop a new catalyst to replace commercial platinum catalysts.[1] In this work,nickel-supported N-doped carbon materials(Ni NPs-N/C)was prepared through hydrothermal method[2].The surface morphology and composition of the Ni NPs-N/C was characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM)and high-resolution transmission electron microscopy(HR-TEM).