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The recovery of rhenium from molybdenite has both important environmental and economic values [1-2].The separation of rhenium from molybdenum in aqueous solution has always been a problem in hydrometallurgy [2].The current industr ial practice of recovery rhenium from rhenium bearing materials can be described as leaching-extraction and leaching-ion exchanging resin absorbing-eluting processes [3-7].The objective of this study was that the separation of rhenium from electric-oxidation lixivium containing rhenium and molybdenum by ion exchanging resin absorbing-eluting processes using D201 resin.The optimum adsorption parameters for Re (Ⅶ) were established as follows:30℃,pH=8,and absorbing time 1 h.